Transmission electron microscopy (TEM)
Analyte
Solid systems;
Composites, materials, organic and inorganic substances, thin layers
Equipment
- Device: JEM-1400Plus (Jeol), accelerating voltage up to 200 kV, digital image recording and filing
Evaluation methods and targets
- Image analysis by image processing software (Olympus GmbH, Germany): determination of particle sizes and their distribution
- Morphology of cross-sections and surfaces with a resolution of up to 10 nm
- Identification of morphological structures in materials from natural and synthetic polymers
- Investigation of structure-property-correlations depending on production and growth parameters, respectively, particularly natural polymers
Application examples
- Ultra thin cross-section of a viscose fiber: core-shell structure with pores (→ Image gallery)
- Surface mark of pulp: fibrillation of the primary wall (→ Image gallery)
- Exfoliation of nanoclays in polymeric matrix