Microscopy

Transmission electron microscopy (TEM)

 

Analyte

Solid systems;
Composites, materials, organic and inorganic substances, thin layers

 

Equipment

  • Device: JEM-1400Plus (Jeol), accelerating voltage up to 200 kV, digital image recording and filing

 

Evaluation methods and targets

  • Image analysis by image processing software (Olympus GmbH, Germany): determination of particle sizes and their distribution
  • Morphology of cross-sections and surfaces with a resolution of up to 10 nm
  • Identification of morphological structures in materials from natural and synthetic polymers
  • Investigation of structure-property-correlations depending on production and growth parameters, respectively, particularly natural polymers

 

Application examples

  • Ultra thin cross-section of a viscose fiber: core-shell structure with pores (→ Image gallery)
  • Surface mark of pulp: fibrillation of the primary wall (→ Image gallery)
  • Exfoliation of nanoclays in polymeric matrix

 

© Fraunhofer IAP
Ultra thin cross-section of a viscose fiber: core-shell structure with pores.
© Fraunhofer IAP
Surface mark of pulp: fibrillation of the primary wall.